SPIN INNING BASKET REACTOR APPARATUS

Product Description

Specification:

SPIN INNING BASKET REACTOR APPARATUS

Description

Any catalytic liquid-liquid orliquid-gas reaction involving the use of a catalyst placed in basket can bestudies in this set-up.

Kinetic parameter of a specificreaction can be estimated & parametric studies can be conducted.

The set-up consists of a reactorcentrally having one spinning basket derived through a variable speed motor.The metered flow of reactant from feed tank is fed to the reactor at thebottom.

The set-up can be used as batch wiseof as continuous type. Sampling points are provided for analysis. Portconnection for gas inlet is provided at the bottom of the reactor

Experimentation/Learning Objectives

To determine the kinetic parametersfor a given reaction

Utilities Required

Electricity Supply: Single Phase, 220 V AC, 50 Hz, 5-15Amp combined socket with earth connection. Earth voltage should be less than 5volts.

Compressed air supply@1 Bar.

Water Supply.

Floor Drain.

Floor Area Required: 1.0 m x 0.75 m.

Instruments, Laboratory Glassware andChemicals required for analysis as per the system adopted

Technical Details

Reactor Vessel: Material Stainless Steel Effective Volume: 1000ml.

Basket: Material Stainless Steel, Fitted with appropriate StainlessSteel.

Drive for Basket: DC Motor with Thyristor controlledDC Drive for Variable Speed.

Packing: Catalyst

Feed Tank (1Nos.): Material Stainless Steel, Capacity10 Ltrs.

Flow Measurement: By Rotameter

Pressure regulator: Range 0-2 kg/cmï

Pressure Gauge: Bourdon Type, 0-2 kg/cmï

Receiver: Material Stainless Steel, Capacity 10 Ltrs.

Piping: Stainless Steel and PVC.

Hot water Circulation: Magnetic Pump of Poly propylene (inouter Jacket) to circulate Hot Water maximum working temp. 85C

Hot water tank: Made of Stainless Steel, Double wall, insulatedwith Ceramic Wool.

Capacity: 10-15 ltrs.