Specification:
BATCH CRYSTALLIZER APPARATUS
Description:
Crystallization is the formation ofsolid particles within a homogeneous phase of saturated liquid.
Its wide use has a two-fold basis, acrystal formed from an impure solution is itself pure and crystallizationaffords a practical method of separating.
This operation involves both heat andmass transfer. Cooling type agitated batch crystallizer set up consists of anopen jacketed stirred vessel provided with water heating & coolingarrangement.
The feed is prepared in thecrystallizer itself with hot water and stirrer. The hot saturated solution inthe crystallizer is then cooled by circulation of cooling water and crystalsare formed.
Experimentation:
To study the performance of a BatchCrystallizer.
To determine the crystal yield andthe efficiency of crystallizer.
Utilities Required:
Water Supply.
Drain.
Electricity Supply: 1 Phase, 220 VAC, 1.5 kW.
Required Chemicals.
Technical Details:
Crystallizer (Jacketed Type): Material Stainless Steel, Cap. 2Ltrs. with conical bottom
Stirrer: FHP, Variable Speed.
Heater: Nichrome wire heater
Cooling Water Tank: Material Stainless Steel, Capacity30 litre fitted with Pump.
Flow measurement: Rotameter for cooling water.
Pump: FHP.
Receiving Tank: Material Stainless Steel , Capacity 2 litre withSS sieve
Temp. Sensors: RTD PT-100 type
Control panel comprises of: Digital Temp. Indicator: 0-199.90Cwith multi-channel switch and Standard make on/off switch, Mains Indicator etc.
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